1.Institute of Applied Physics, Abbe Center of Photonics, Friedrich-Schiller-Universität Jena, Albert-Einstein-Str. 15, 07745, Jena, Germany
2.Helmholtz-Institute Jena, Fröbelstieg 3, 07743, Jena, Germany
3.Leibniz Institute of Photonic Technology, Albert-Einstein-Straße 9, 07745, Jena, Germany
4.Fraunhofer Institute for Microstructure of Materials and Systems IMWS, Walter-Hülse-Str. 1, 06120, Halle, Germany
5.Fraunhofer Institute for Applied Optics and Precision Engineering IOF, Albert-Einstein-Str. 7, 07745, Jena, Germany
Wilhelm Eschen (wilhelm.eschen@uni-jena.de)
纸质出版日期:2022-05-31,
网络出版日期:2022-04-29,
收稿日期:2022-01-18,
修回日期:2022-04-07,
录用日期:2022-04-11
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Material-specific high-resolution table-top extreme ultraviolet microscopy[J]. LSA, 2022,11(5):991-1000.
Eschen, W. et al. Material-specific high-resolution table-top extreme ultraviolet microscopy. Light: Science & Applications, 11, 991-1000 (2022).
Material-specific high-resolution table-top extreme ultraviolet microscopy[J]. LSA, 2022,11(5):991-1000. DOI: 10.1038/s41377-022-00797-6.
Eschen, W. et al. Material-specific high-resolution table-top extreme ultraviolet microscopy. Light: Science & Applications, 11, 991-1000 (2022). DOI: 10.1038/s41377-022-00797-6.
Microscopy with extreme ultraviolet (EUV) radiation holds promise for high-resolution imaging with excellent material contrast
due to the short wavelength and numerous element-specific absorption edges available in this spectral range. At the same time
EUV radiation has significantly larger penetration depths than electrons. It thus enables a nano-scale view into complex three-dimensional structures that are important for material science
semiconductor metrology
and next-generation nano-devices. Here
we present high-resolution and material-specific microscopy at 13.5 nm wavelength. We combine a highly stable
high photon-flux
table-top EUV source with an interferometrically stabilized ptychography setup. By utilizing structured EUV illumination
we overcome the limitations of conventional EUV focusing optics and demonstrate high-resolution microscopy at a half-pitch lateral resolution of 16 nm. Moreover
we propose mixed-state orthogonal probe relaxation ptychography
enabling robust phase-contrast imaging over wide fields of view and long acquisition times. In this way
the complex transmission of an integrated circuit is precisely reconstructed
allowing for the classification of the material composition of mesoscopic semiconductor systems.
Wagner, C.&Harned, N. EUV lithography: lithography gets extreme.Nat. Photonics4, 24–26 (2010)..
Priolo, F. et al. Silicon nanostructures for photonics and photovoltaics.Nat. Nanotechnol.9, 19–32 (2014)..
Sun, Y. M., Liu, N.&Cui, Y. Promises and challenges of nanomaterials for lithium-based rechargeable batteries.Nat. Energy1, 16071 (2016)..
Staude, I.&Schilling, J. Metamaterial-inspired silicon nanophotonics.Nat. Photonics11, 274–284 (2017)..
Bogaerts, W. et al. Programmable photonic circuits.Nature586, 207–216 (2020)..
Kauffman, R. L., Phillion, D. W.&Spitzer, R. C. X-ray production ~13 nm from laser-produced plasmas for projection x-ray lithography applications.Appl. Opt.32, 6897–6900 (1993)..
Torretti, F. et al. Prominent radiative contributions from multiply-excited states in laser-produced tin plasma for nanolithography.Nat. Commun.11, 2334 (2020)..
Barbee, T. W., Mrowka, S.&Hettrick, M. C. Molybdenum-silicon multilayer mirrors for the extreme ultraviolet.Appl. Opt.24, 883–886 (1985)..
Chkhalo, N. I. et al. High-reflection Mo/Be/Si multilayers for EUV lithography.Opt. Lett.42, 5070–5073 (2017)..
Miao, J. W. et al. Beyond crystallography: diffractive imaging using coherent X-ray light sources.Science348, 530–535 (2015)..
Brizuela, F. et al. Microscopy of extreme ultraviolet lithography masks with 13.2 nm tabletop laser illumination.Opt. Lett.34, 271–273 (2009)..
Wang, S. et al. Single-shot large field of view Fourier transform holography with a picosecond plasma-based soft X-ray laser.Opt. Express28, 35898–35909 (2020)..
Brewer, C. A. et al. Single-shot extreme ultraviolet laser imaging of nanostructures with wavelength resolution.Opt. Lett.33, 518–520 (2008)..
Kördel, M. et al. Laboratory water-window x-ray microscopy.Optica7, 658–674 (2020)..
Pupeza, I. et al. Extreme-ultraviolet frequency combs for precision metrology and attosecond science.Nat. Photonics15, 175–186 (2021)..
Popmintchev, T. et al. Bright coherent ultrahigh harmonics in the keV X-ray regime from mid-infrared femtosecond lasers.Science336, 1287–1291 (2012)..
Klas, R. et al. Ultra-short-pulse high-average-power megahertz-repetition-rate coherent extreme-ultraviolet light source.PhotoniX2, 4 (2021)..
Duarte, J. et al. Computed stereo lensless X-ray imaging.Nat. Photonics13, 449–453 (2019)..
Zayko, S. et al. Ultrafast high-harmonic nanoscopy of magnetization dynamics.Nat. Commun.12, 6337 (2021)..
Bartels, R. A. et al. Generation of spatially coherent light at extreme ultraviolet wavelengths.Science297, 376–378 (2002)..
Thibault, P. et al. High-resolution scanning X-ray diffraction microscopy.Science321, 379–382 (2008)..
Maiden, A. M.&Rodenburg, J. M. An improved ptychographical phase retrieval algorithm for diffractive imaging.Ultramicroscopy109, 1256–1262 (2009)..
Seaberg, M. D. et al. Tabletop nanometer extreme ultraviolet imaging in an extended reflection mode using coherent Fresnel ptychography.Optica1, 39–44 (2014)..
Gardner, D. F. et al. Subwavelength coherent imaging of periodic samples using a 13.5 nm tabletop high-harmonic light source.Nat. Photonics11, 259–263 (2017)..
Baksh, P. D. et al. Quantitative and correlative extreme ultraviolet coherent imaging of mouse hippocampal neurons at high resolution.Sci. Adv.6, eaaz3025 (2020)..
Tanksalvala, M. et al. Nondestructive, high-resolution, chemically specific 3D nanostructure characterization using phase-sensitive EUVimaging reflectometry.Sci. Adv.7, eabd9667 (2021)..
Odstrcil, M. et al. Ptychographic coherent diffractive imaging with orthogonal probe relaxation.Opt. Express24, 8360–8369 (2016)..
Thibault, P.&Menzel, A. Reconstructing state mixtures from diffraction measurements.Nature494, 68–71 (2013)..
Grebing, C. et al. Kilowatt-average-power compression of millijoule pulses in a gas-filled multi-pass cell.Opt. Lett.45, 6250–6253 (2020)..
Tadesse, G. K. et al. Wavelength-scale ptychographic coherent diffractive imaging using a high-order harmonic source.Sci. Rep.9, 1735 (2019)..
Enders, B.Development and Application of Decoherence Models in Ptychographic Diffraction Imaging. PhD thesis, Technical University Munich (2016).
Maiden, A. M., Rodenburg, J. M.&Humphry, M. J. Optical ptychography: a practical implementation with useful resolution.Opt. Lett.35, 2585–2587 (2010)..
Guizar-Sicairos, M. et al. Role of the illumination spatial-frequency spectrum for ptychography.Phys. Rev. B86, 100103 (2012)..
Odstrčil, M. et al. Towards optimized illumination for high-resolution ptychography.Opt. Express27, 14981–14997 (2019)..
Maiden, A. M. et al. Soft X-ray spectromicroscopy using ptychography with randomly phased illumination.Nat. Commun.4, 1669 (2013)..
Baksh, P. D. et al. Wide-field broadband extreme ultraviolet transmission ptychography using a high-harmonic source.Opt. Lett.41, 1317–1320 (2016)..
Loetgering, L. et al. Tailoring spatial entropy in extreme ultraviolet focused beams for multispectral ptychography.Optica8, 130–138 (2021)..
Heckenberg, N. R. et al. Generation of optical phase singularities by computer-generated holograms.Opt. Lett.17, 221–223 (1992)..
Fanciulli, M. et al. Observation of magnetic helicoidal dichroism with extreme ultraviolet light vortices.Phys. Rev. Lett.128, 077401 (2022)..
Loetgering, L. et al. Generation and characterization of focused helical x-ray beams.Sci. Adv.6, eaax8836 (2020)..
Vila-Comamala, J. et al. Characterization of high-resolution diffractive X-ray optics by ptychographic coherent diffractive imaging.Opt. Express19, 21333–21344 (2011)..
van Heel, M.&Schatz, M. Fourier shell correlation threshold criteria.J. Struct. Biol.151, 250–262 (2005)..
Jones, M. W. M. et al. Mapping biological composition through quantitative phase and absorption X-ray ptychography.Sci. Rep.4, 6796 (2014)..
Henke, B. L., Gullikson, E. M.&Davis, J. C. X-ray interactions: photoabsorption, scattering, transmission, and reflection atE= 50–30, 000 eV,Z= 1–92.At. Data Nucl. Data Tables54, 181–342 (1993)..
Loetgering, L. et al. ptyLab: a cross-platform inverse modeling toolbox for conventional and Fourier ptychography. inProceedings of the OSA Imaging and Applied Optics Congress 2021(Optical Society of America, 2021).
Yao, Y. et al. Broadband X-ray ptychography using multi-wavelength algorithm.J. Synchrotron Radiat.28, 309–317 (2021)..
Shapiro, D. A. et al. An ultrahigh-resolution soft x-ray microscope for quantitative analysis of chemically heterogeneous nanomaterials.Sci. Adv.6, eabc4904 (2020)..
Willems, F. et al. Magneto-optical functions at the 3presonances of Fe, Co, and Ni: ab initio description and experiment.Phys. Rev. Lett.122, 217202 (2019)..
Zürch, M. et al. Strong-field physics with singular light beams.Nat. Phys.8, 743–746 (2012)..
Hernández-García, C. et al. Attosecond extreme ultraviolet vortices from high-order harmonic generation.Phys. Rev. Lett.111, 083602 (2013)..
Kong, F. Q. et al. Controlling the orbital angular momentum of high harmonic vortices.Nat. Commun.8, 14970 (2017)..
Gauthier, D. et al. Tunable orbital angular momentum in high-harmonic generation.Nat. Commun.8, 14971 (2017)..
Shen, Y. J. et al. Optical vortices 30 years on: OAM manipulation from topological charge to multiple singularities.Light.: Sci. Appl.8, 90 (2019)..
Wang, B. et al. Coherent Fourier scatterometry using orbital angular momentum beams for defect detection.Opt. Express29, 3342–3358 (2021)..
van Veenendaal, M.&McNulty, I. Prediction of strong dichroism induced by X rays carrying orbital momentum.Phys. Rev. Lett.98, 157401 (2007)..
Pronin, O. et al. Ultrabroadband efficient intracavity XUV output coupler.Opt. Express19, 10232–10240 (2011)..
Klas, R. et al. Generation of coherent broadband high photon flux continua in the XUV with a sub-two-cycle fiber laser.Opt. Express28, 6188–6196 (2020)..
Huang, X. J. et al. Optimization of overlap uniformness for ptychography.Opt. Express22, 12634–12644 (2014)..
Thibault, P. et al. Probe retrieval in ptychographic coherent diffractive imaging.Ultramicroscopy109, 338–343 (2009)..
Enders, B.&Thibault, P. A computational framework for ptychographic reconstructions.Proc. R. Soc. A: Math., Phys. Eng. Sci.472, 20160640 (2016)..
Maiden, A., Johnson, D.&Li, P. Further improvements to the ptychographical iterative engine.Optica4, 736–745 (2017)..
Odstrčil, M.Coherent Diffractive Imaging Using Table-top Sources. PhD thesis, University of Southampton (2017).
Goodman, J. W.Introduction to Fourier Optics3rd edn (Roberts&Company Publishers, 2005).
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